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Column:BeksichFluosil5um250x2mm,流速:0.3ml/min溫度:25℃,進(jìn)樣量:10um流動(dòng)相:A:0,1%H3PO4(85%)/49,9%water/MeCN(v/v/v),B:0,1H3PO4(85%)inwaterCatechins:兒茶素；兒茶酚

Column:BeksichStPolyamine,5um(53x4.6mm)流動(dòng)相:A=20mMTRIS-pH7B=1MNH4OAc-pH7梯度:0-100%Bin20min.監(jiān)測波長:280nm,流速:1ml/minLactoglobuline:乳球蛋白BSA:牛血清白蛋白cytochrome細(xì)胞色素

Column:BeksichGTurbo100ODS,1.5um(33x4.6mm)流動(dòng)相:ACN/0,1%TFA(35/65),流速:1.5ml/min.Benzodiazepine苯二氮1=Clonazepam氯*/氯硝安定2=Diazepam安定

Columns:150x4.6mmEluent:MeCN/50mMKH2PO450/50,pH3,Flowrate:1ml/min1:primidone:普里米酮；去氧；撲癇酮2:Phenobarbitone:3:carbamazepine卡馬西平,立痛定；卡巴咪嗪；酰胺咪嗪；氨甲酰氮草

BeksichSt120BS-C23,(100x4.6mm)流動(dòng)相:A=0.1%TFA,B=0,1%TFAinACN梯度:15-40%Bin10min.,流速:1ml/min監(jiān)測波長：230nm

同時(shí)分析1-ａnd2-val.陽離子Column:BeksichCat,5um(or7um)(125x4.6mm)Eluent:5.0mM檸檬酸+0.5mM2,6吡啶二甲酸or0.6mM抗壞血酸+3.3mM磷酸pH2,7

AnioneswithSuppressorColumn:BeksichGelAXS(150x4mm)Eluent:1.7mM碳酸氫鈉/1.8mM碳酸鈉/0.1mM硫氰酸鈉溫度:RT流速:2ml/min.進(jìn)樣量:100ulF：氟離子，Cl：氯離子，Nitrite：亞硝酸鹽，Bromide：溴化物，nitrate；硝酸，Phosphate：磷酸鹽，Sulfate：硫酸Column:BeksichGelAX,10um(150x4mm)Eluent:mM鄰苯二甲酸氫鉀(pH6.0)流...